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Furthermore, a “one-pot” reaction sequence necessitates compatibility between the products formed in each step and the reagents used in subsequent steps. One pot multistep strategy allows for the regioselectivity of the reaction to be controlled during the epoxidation and/or the epoxide ring opening steps.Ī stepwise approach to the oxidative cleavage of alkene C=C bonds faces three main challenges 1) generating the epoxide, 2) selective ring open to the diol and 3) selective oxidation of the diol. A further point with regard to selectivity lies at the ring opening step, which has been largely neglected to date. In a stepwise approach the selectivity towards the C=C bonds to be oxidized is governed by the epoxidation step, and hence a multistep oxidation protocol allows regioselectivity between several alkene motifs to be achieved (Scheme 2). Despite limitations imposed by epoxide ring opening with sulfuric acid, the epoxidation opens up opportunities in regard to the regio- and chemo-selectivity of the system. Epoxidation with an Fe(II) catalyst and the terminal oxidant H 2O 2 was followed by sulfuric acid catalyzed ring opening and finally, cleavage of the trans-diol with stoichiometric NaIO 4 to yield the corresponding (di)carbonyl compounds in good to excellent yields (43 to 99 %) and selectivities (Scheme 1d). 11 reported a one-pot three step epoxidation-dihydroxylation-cleavage, which is equivalent to cleavage with ozone. 9 reported the cleavage of epoxides to carbonyl compounds with aqueous NaIO 4 at room temperature. Ochiai, 26 Lai 27 and co-workers have reported a multi-step one-pot cleavage of alkenes with iodosyl benzene and a manganese porphyrin catalyst, noting that epoxides were formed as intermediates in the reaction. Recently alternative multistep approaches that replace 2 nd and 3 rd row transition metal-based catalysts have been developed. 10, 18, 21- 23 Later, RuCl 3 was used in combination with NaIO 4 or Oxone, with various solvent combinations, to give the similar transformations. This approach is used widely despite the cost and toxicity of OsO 4. 18- 20 Lemieux and Johnson's method (Scheme 1c) for alkene double bond cleavage employs catalytic OsO 4 to form the diol intermediate and NaIO 4 both as terminal oxidant to regenerate the osmium tetroxide and to cleave the diol formed. One pot methods 17 using catalytic RuCl 3 or OsO 4 in combination with either Oxone TM, NaOCl, or NaIO 4, directly exploit the ability of the oxidant to cleave the oxidation products formed by the catalytic first step. ![]() 10 (d) 3-step epoxidation-ring opening-cleavage strategy developed by Klein Gebbink et al. (a) Diol C–C bond cleavage with NaIO 4, (b) C–C bond cleavage in 3-carene oxide by Binder et al. via epoxidation, can be followed by C–C bond cleavage with NaIO 4 or HIO 4, with often high selectivity and typically full conversion (Scheme 1), 12, 13 which outweighs the “single step” benefit of direct treatment of alkenes with ozone, Cr 2O 7 2– or MnO 4 –. ![]() For instance, initial conversion of alkenes to vic-diols, e.g. Stepwise approaches can provide increased selectivity, as they allow greater control over the conditions in each step. In particular, the avoidance of uncontrolled over oxidation of the products is challenging. Furthermore, scale-up opportunities are limited by the low temperatures, typically from – 78 to 0 ☌ 5- 8 and functional group intolerance, e.g., alkynes are converted to carboxylic acids.Ī key challenge in non-ozone based methods for C=C bond cleavage is to achieve the good atom economy and selectivity that can be achieved with ozonolysis. Flow chemistry 4 can reduce the steady state concentrations of O 3, however, the latter risks are not mitigated by this approach. 2, 3 Its versatility is such that it is used widely, despite that alkene ozonolysis creates hazards in the in situ generation of O 3, and the presence of ozonides and peroxides during concentration steps. 1 For example, ozonolysis, provides access to wide range of products controlled largely by the conditions used and the fate of the trioxolane intermediate. Cleavage of the double bonds of alkenes to yield (di)carbonyl compounds (ketones and aldehydes) is a key reaction in synthetic organic chemistry and especially in total synthesis and medicinal chemistry. Heck, it may even inspire you to write your own book. 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![]() During his time at ANSTO, Adi had strategic oversight and responsibility for ANSTO’s multi-faceted portfolio of activities, including securing funding and operating the Australian Synchrotron, a major research facility serving as an innovation hub in southeast Melbourne.Prior to founding Siyeva in 2021, Adi worked as the CEO for Australia’s Nuclear Science and Technology Organization (ANSTO), one of Australia’s largest public research organizations and recognized as an international player in nuclear science and technology.Adi Paterson is the Principal and Founder of Siyeva Consulting.Brian graduated cum laude from Princeton University with an A.B.Brian started his career at Merrill Lynch in New York, where he worked in the financial sponsors and energy & power groups in the investment banking division.While at First Reserve, Brian worked on several co-investments with AMCI, including the formation of AMCI Capital L.P. Prior to joining AMCI, Brian worked at First Reserve Corporation, a leading private equity firm specializing in the energy industry.Brian has served on the Boards of Directors of 14 companies during his time at AMCI, and has served on the Board of Jupiter Mines Ltd (ASX: JMS) since October 2019.Brian was an officer of AMCI Acquisition Corp., a SPAC that successfully completed a business combination with Advent Technologies, Inc.Since Brian joined the Investment Committee at AMCI, AMCI has invested $1.6 billion of its capital and approximately $0.7 billion of co-investor capital across the global industrial, transportation and natural resources sectors.Brian is a Managing Director, Co-head of Investments and a member of the Investment Committee for AMCI Group.from the Wharton School of the University of Pennsylvania Nimesh graduated cum laude from Princeton University with an A.B.Previously Nimesh was with ChrysCapital, where he focused on private equity investments in the technology-enabled services, business process outsourcing and renewable energy sectors.Prior to joining AMCI, Nimesh was with Great Hill Partners where he focused on private equity investments in technology-enabled services companies.Nimesh has served on the Boards of Directors or represented AMCI’s equity interests in 8 companies during his time at AMCI.Nimesh was an officer of AMCI Acquisition Corp., a SPAC that successfully completed a business combination with Advent Technologies, Inc.Since Nimesh joined the Investment Committee at AMCI, AMCI has invested $1.4 billion of its capital and approximately $0.5 billion of co-investor capital across the global industrial, transportation and natural resources sectors.Nimesh is a Managing Director, Co-head of Investments and a member of the Investment Committee for AMCI Group. ![]() ![]() ActiveState also provides business solutions of dynamic languages, including enterprise distributions and OEM licensing, that offer guaranteed stability, expert support, unparalleled quality and cost-efficiency to organizations. 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Marie embraces slower experimental composition on pieces like Kidnap You in the Desert, Insomnie, and Perséphone, while songs like Excès de Vitesse and Balade aux USA are decidedly upbeat and indicate a broadening complexity in Marie's aesthetic domain. However, 2015's Un Autre Voyage bares the immense weight of Davidson's psyche by turning direct experience into song, utilizing her candid self-examination to convey a new found serenity that playfully underlines her otherwise brooding and pensive soundscapes. In 2014's Perte d'Identité (Weyrd Son) Davidson narrates her search for self through the course of trial and conquest, establishing her distinct method of song writing that is as compelling as it is existential. This stands in stark contrast to Davidson's self-titled debut EP (HOLODECK, 2013), which depicts a disoriented mind struggling for stability throughout a period of depression in her musical and personal life. Through this concerted disclosure, Marie's unique practice of surreal atmospheric composition now shows irrepressible traces of exuberance, displaying a fresh luminosity in her emotive palette. This act of self-journalism serves as a psychological cleansing that evokes an authentic sense of warmth and empathy, rendering Un Autre Voyage as Davidson's most transparently honest artistic document yet. Un Autre Voyage (translated as "Another Journey") is a collection of songs based solely on true events, providing the listener with an unfiltered primary account of Marie's intrapersonal experiences. Davidson's third album Un Autre Voyage demonstrates her heightened compositional skill behind a sequencer as well as her singular ability to anesthetize the senses through the documentation of her own serial pattern of experiential growth. Davidson's intimate solo work is embodied through a host of synthesizers and drum machines that coalesce in synchronized harmony, punctuated by Marie's hypnotic vocal delivery, sung and spoken in both French and English. In 2012 Marie began to unveil compositions under her own name, revealing a solo artist who possessed the confident vulnerability required to write, produce, and perform unaccompanied. As a long-time member of Les Momies de Palerme, Hotel Monochrome, DKMD, and Essaie Pas, Marie has continued to hone her many talents in Montréal's fervent experimental communities for much of her adult life. From the prolific cultural epicenter of Montréal, Marie Davidson has emerged as one of the foremost electronic artists in contemporary underground pop today. ![]() Then the app will automatically apply the edits made to the selected images.īatchPhoto offers you two ways to crop your pictures: Auto Crop and Crop. 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You can easily do this by dragging the edges of the selection rectangle. Photos is a built-in image editor that comes with a series of useful features, including the ability to crop images. Since you’re an Apple user, why not first try something Apple itself developed for image editing? Therefore, in this article we’ve compiled a list of easy-to-use, budget-friendly Mac apps which satisfy your need of efficiently cropping pictures. Naturally, the first name that comes to mind is Photoshop, but the program is pretty costly and rather designed for more complex editing, not for such a basic task. Why? Well, simply because there are numerous ways this operation can help you create quality images.īy cropping you can improve the overall composition of the image, you can change the aspect ratio, as well as remove unnecessary, distraction-causing parts in order to maintain the focus on the main subject.Ĭropping is without a doubt useful in many situations and this is the reason why it’s basically ubiquitous – almost all photo editing software offer this feature. Place your resized videos in any location from IGTV to TikTok without cutting off important parts, leaving bars on the sides, or having distracting watermarks interfere.Cropping is many times an integral part of the photo editing process. If you want to resize your video to exact dimensions, you can use the Studio to input exact pixels for your video's aspect ratio, so it can fit perfectly wherever you want to use it. 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